Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

Base Information

Chemical Name:Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester
CAS No.:143326-06-1
Molecular Formula:C₅₉H₉₈NO₁₇P
Molecular Weight:1124.4
Hs Code.:

Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

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Chemical Property of Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

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Technology Process of Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

There total 4 articles about Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143326-05-0,143393-19-5,143393-20-8,143393-21-9
Benzoic acid 1-{2-[(2-cyano-ethoxy)-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

: 143326-06-1,143393-22-0
Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

Guidance literature:: With tert-butylamine; at 20 ℃; for 0.5h; Yield given;
DOI:10.1016/S0040-4039(00)92684-4

Reference yield:

: 41899-51-8
rac-3-Benzoylceramide

: 143326-06-1,143393-22-0
Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / diisopropylammonium tetrazolide / CH₂Cl₂

2: 90 percent Spectr_. / 1H-tetrazole / acetonitrile; CH₂Cl₂ / 0.25 h

3: t-BuO₂H

4: t-BuNH₂ / 0.5 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; N,N-diisopropylamine tetrazolide; tert-butylamine; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)92684-4

Reference yield:

: 139472-73-4,143393-12-8,143393-13-9
Benzoic acid 1-{2-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

: 143326-06-1,143393-22-0
Benzoic acid 1-{2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentaacetoxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoylamino-ethyl}-hexadecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent Spectr_. / 1H-tetrazole / acetonitrile; CH₂Cl₂ / 0.25 h

2: t-BuO₂H

3: t-BuNH₂ / 0.5 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; tert-butylamine; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)92684-4