Technology Process of C14(13)CH17NO2
There total 3 articles about C14(13)CH17NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78 percent / H2, AcONa / Adams catalyst / methanol / 3 h / Ambient temperature
2: POCl3 / CH2Cl2 / 0.5 h / Heating
3: 1.0 M BH3*THF / 1,2-dimethoxy-ethane; tetrahydrofuran / 68 h / Ambient temperature
With
borane-THF; hydrogen; sodium acetate; trichlorophosphate;
platinum(IV) oxide;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: POCl3 / CH2Cl2 / 0.5 h / Heating
2: 1.0 M BH3*THF / 1,2-dimethoxy-ethane; tetrahydrofuran / 68 h / Ambient temperature
With
borane-THF; trichlorophosphate;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;
- Guidance literature:
-
With
borane-THF;
In
tetrahydrofuran; 1,2-dimethoxyethane;
for 68h;
Yield given. Yields of byproduct given;
Ambient temperature;