6-Chloro-2,3-bis(chloromethyl)pyridine

Base Information

Chemical Name:6-Chloro-2,3-bis(chloromethyl)pyridine
CAS No.:220001-94-5
Molecular Formula:C₇H₆Cl₃N
Molecular Weight:210.49
Hs Code.:
DSSTox Substance ID:DTXSID80460168
Wikidata:Q82284118
Mol file:220001-94-5.mol

Synonyms:6-chloro-2,3-bis(chloromethyl)pyridine;220001-94-5;Pyridine, 6-chloro-2,3-bis(chloromethyl)-;SCHEMBL3885727;DTXSID80460168;XQMVICDINIHBII-UHFFFAOYSA-N;AKOS016845023;2-chloro-5,6-di(chloromethyl)pyridine;6-chloro-2,3-bis-chloromethyl-pyridine;N13342;J-518512

Suppliers and Price of 6-Chloro-2,3-bis(chloromethyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
6-Chloro-2,3-bis(chloromethyl)pyridine 95+%
1g
$ 580.00

Chemenu
6-Chloro-2,3-bis(chloromethyl)pyridine 95%
1g
$ 542.00

American Custom Chemicals Corporation
6-CHLORO-2,3-BIS-(CHLOROMETHYL)PYRIDINE 95.00%
5MG
$ 500.12

Alichem
6-Chloro-2,3-bis(chloromethyl)pyridine
1g
$ 614.80

Total 3 raw suppliers

Chemical Property of 6-Chloro-2,3-bis(chloromethyl)pyridine

Chemical Property:

Storage Temp.:2-8°C
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:208.956582
Heavy Atom Count:11
Complexity:120

Purity/Quality:

95+% ^*data from raw suppliers

6-Chloro-2,3-bis(chloromethyl)pyridine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=NC(=C1CCl)CCl)Cl

Technology Process of 6-Chloro-2,3-bis(chloromethyl)pyridine

There total 5 articles about 6-Chloro-2,3-bis(chloromethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 220001-93-4
(6-chloropyridine-2,3-diyl)dimethanol

: 220001-94-5
6-chloro-2,3-bis(chloromethyl)pyridine

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h;

Reference yield:

: 605-38-9
dimethyl 2,3-pyridinedicarboxylate

: 220001-94-5
6-chloro-2,3-bis(chloromethyl)pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: urea hydrogen peroxide adduct / acetonitrile / 3 h / 0 - 20 °C

2: trichlorophosphate / 3 h / 105 °C

3: methanol; lithium borohydride / tetrahydrofuran / 2.5 h / 20 °C / Cooling with ice

4: thionyl chloride / 3 h / 20 °C

With methanol; lithium borohydride; thionyl chloride; urea hydrogen peroxide adduct; trichlorophosphate; In tetrahydrofuran; acetonitrile;

Reference yield:

: 32383-02-1
pyridine-2,3-dicarboxylic acid dimethyl ester N-oxide

: 220001-94-5
6-chloro-2,3-bis(chloromethyl)pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 3 h / 105 °C

2: methanol; lithium borohydride / tetrahydrofuran / 2.5 h / 20 °C / Cooling with ice

3: thionyl chloride / 3 h / 20 °C

With methanol; lithium borohydride; thionyl chloride; trichlorophosphate; In tetrahydrofuran;