[RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl

Base Information

Chemical Name:[RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl
CAS No.:1264748-67-5
Molecular Formula:C₂₀H₃₀ClN₃Rh*Cl
Molecular Weight:486.29
Hs Code.:

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Chemical Property of [RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl

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Technology Process of [RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl

There total 1 articles about [RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 38435-15-3
Me₂NNC(Ph)NHMe

: 1264748-67-5
[RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl

Guidance literature:: In dichloromethane; (inert atm.); mixing CH2Cl2 solns. of rhodium compd. and hydrazine deriv., stirring at room temp. for 48 h; concg., addn. of pentane, filtration, washing with pentane, NMR and MS;
DOI:10.1039/c0dt01267j

Reference yield: 77.0%

: 1264748-67-5
[RhCl(C5Me5)(Me2NNHC(Ph)NMe-κ2N1,N3)]Cl

: 1264748-70-0
[RhCl(C5Me5)(Me2NNC(Ph)NMe-κ2N1,N3)]

Guidance literature:: With LiN(Si(CH₃)3)2; In toluene; (inert atm.); addn. of toluene soln. of 1 equiv. of lithium amide deriv.to toluene soln. of rhodium compd., keeping at room temp. for 2 h; filtration, concg., addn. of pentane, filtration, washing with pentane, NMR and MS;
DOI:10.1039/c0dt01267j