benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate

Base Information

Chemical Name:benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate
CAS No.:1300087-14-2
Molecular Formula:C₂₆H₂₃N₅O₂
Molecular Weight:437.501
Hs Code.:

Synonyms:

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Chemical Property of benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate

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Technology Process of benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate

There total 9 articles about benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300089-50-2
benzyl (8-methyl-5-phenyl-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)carbamate

: 1300087-14-2
benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol / 16 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3: acetic acid / 0.5 h / Reflux

With hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jm401088k

Reference yield:

: C₃₀H₂₆N₆O₃

: 1300087-14-2
benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium acetate; acetic acid / 24 h / 20 °C

2: Lawessons reagent / toluene / 4 h / Reflux

3: hydrazine hydrate / methanol / 16 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5: acetic acid / 0.5 h / Reflux

With Lawessons reagent; ammonium acetate; hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/jm401088k

Reference yield:

: [benzotriazol-1-yl-(2-benzoyl-5-methyl-phenylcarbamoyl)-methyl]-carbamic acid benzyl ester

: 1300087-14-2
benzyl (1,9-dimethyl-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: ammonia / methanol / 1 h / 20 °C / Inert atmosphere

2: ammonium acetate; acetic acid / 24 h / 20 °C

3: Lawessons reagent / toluene / 4 h / Reflux

4: hydrazine hydrate / methanol / 16 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

6: acetic acid / 0.5 h / Reflux

With Lawessons reagent; ammonium acetate; ammonia; hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/jm401088k