(CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2

Base Information

Chemical Name:(CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2
CAS No.:148510-19-4
Molecular Formula:C₂₉H₂₃CrO₅PSn
Molecular Weight:653.178
Hs Code.:

(CO)5CrC<sub>6</sub>H<sub>5</sub>P(C<sub>6</sub>H<sub>5</sub>CCH)2Sn(CH<sub>3</sub>)2

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Chemical Property of (CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2

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Technology Process of (CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2

There total 2 articles about (CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 72868-71-4
phenylphosphine pentacarbonylchromium⁽⁰⁾

: 3912-89-8
di(phenylethyn-1-yl)dimethylstannane

: 148510-19-4
(CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2

: 148510-24-1
(CO)5CrC₆H₅PHCC₆H₅CHSn(CH₃)2CCC₆H₅

Guidance literature:: With azoisobutyronitrile; In toluene; (N2); dry and fresh distd. solvents; stirring Cr-compd. and Me2Sn(CCPh)2 in the presence of AIBN in toluene at 60°C (16 h);; removal of volatile components in vac., chromy. (SiO2, petroleum ether/CH2Cl2 5:1) at -20°C, removal of solvent in vac., recrystn. (n-pentane, toluene); elem. anal.;;
DOI:10.1016/0022-328X(93)83054-Y

Reference yield:

: 72868-71-4
phenylphosphine pentacarbonylchromium⁽⁰⁾

: 3912-89-8
di(phenylethyn-1-yl)dimethylstannane

: 148510-19-4
(CO)5CrC₆H₅P(C₆H₅CCH)2Sn(CH₃)2

Guidance literature:: Multi-step reaction with 2 steps

1: azoisobutyronitrile / toluene

2: azoisobutyronitrile / toluene

With azoisobutyronitrile; In toluene;
DOI:10.1016/0022-328X(93)83054-Y