4',4'''-azoxybis

Base Information

• Chemical Name: 4',4'''-azoxybis
• CAS No.: 150195-97-4
• Molecular Formula: C₂₆H₁₆Cl₂N₂O₃
• Molecular Weight: 475.331

Synonyms:

Chemical Property of 4',4'''-azoxybis

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4',4'''-azoxybis

There total 2 articles about 4',4'''-azoxybis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4',4'''-azoxybis → 4',4'''-azoxybis (150195-97-4)

Guidance literature:

With phosphorus pentachloride; trichlorophosphate; 1.) r.t., 4 h, 2.) to 60 deg C;

DOI:10.1002/recl.19931120606

Reference yield:

4'-nitro-biphenyl-4-carboxylic acid (92-89-7) → 4',4'''-azoxy-bis-biphenyl-4-carbonyl chloride (150195-97-4)

Guidance literature:

ueber <4.4''>Azoxybiphenyl-dicarbonsaeure-(4'.4''');

Reference yield: 38.0%

1-bromo-6-hexanol (4286-55-9) + 4',4'''-azoxybis (150195-97-4) → 4',4'''-azoxybis (150195-96-3)

Guidance literature:

With triethylamine; In 1,2-dichloro-benzene; Ambient temperature;

DOI:10.1002/recl.19931120606

upstream raw materials:

4'-nitro-biphenyl-4-carboxylic acid

Downstream raw materials:

4',4'''-azoxybis

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