tris(triphenylphosphine)silver(I) pentafluoropropionate

Base Information

• Chemical Name: tris(triphenylphosphine)silver(I) pentafluoropropionate
• CAS No.: 667423-27-0
• Molecular Formula: C₅₇H₄₅AgF₅O₂P₃
• Molecular Weight: 1057.76
• Mol file: 667423-27-0.mol

Synonyms:

Chemical Property of tris(triphenylphosphine)silver(I) pentafluoropropionate

Chemical Property:

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Technology Process of tris(triphenylphosphine)silver(I) pentafluoropropionate

There total 1 articles about tris(triphenylphosphine)silver(I) pentafluoropropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.7%

silver(I) pentafluoropropionate (509-09-1) + triphenylphosphine (603-35-0) → tris(triphenylphosphine)silver(I) pentafluoropropionate (667423-27-0)

Guidance literature:

In dichloromethane; under N2; soln. of PPh3 in CH2Cl2 slowly added to suspn. of C2F5CO2Ag inCH2Cl2 at 40°C (molar ratio = 3:1); after 2 h mixt. concd.; cold pentane (-70°C) added; ppt. recrystd. from THF/pentane; elem. anal.;

DOI:10.1016/S0020-1693(03)00468-7

upstream raw materials:

silver(I) pentafluoropropionate

triphenylphosphine