2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide

Base Information

• Chemical Name: 2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide
• CAS No.: 604809-72-5
• Molecular Formula: C₅₈H₈₁N₇O₁₂S₂
• Molecular Weight: 1132.45

Synonyms:

Chemical Property of 2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide

Chemical Property:

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Technology Process of 2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide

There total 1 articles about 2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[2-(2-{2-[2-(2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-3-tert-butoxy-butyrylamino)-3-mercapto-propionylamino]-propionylamino}-3-phenyl-propionylamino)-3-methyl-pentanoylamino]-4-methylsulfanyl-butyric acid → 2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide (604809-72-5)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; N-polystyrene methyl-N'-cyclohexylcarbodiimide; In chloroform; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/S0960-894X(03)00497-9

Reference yield:

2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide (604809-72-5) → N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-2-{2-[4-(4-benzyl-phenoxy)-butyrylamino]-3-hydroxy-propionylamino}-3-hydroxy-butyramide

Guidance literature:

With triethylsilane; Ethyl methyl sulfide; trifluoroacetic acid;

DOI:10.1016/S0960-894X(03)00497-9

Reference yield:

2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-tert-butoxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-tert-butoxy-butyramide (604809-72-5) → 2-{2-[4-(4-benzoyl-phenoxy)-butyrylamino]-3-hydroxy-propionylamino}-N-[9-benzyl-6-sec-butyl-12-methyl-3-(2-methylsulfanyl-ethyl)-2,5,8,11,14-pentaoxo-1-thia-4,7,10,13-tetraaza-cyclohexadec-15-yl]-3-hydroxy-butyramide

Guidance literature:

With Ethyl methyl sulfide; chlorotriisopropylsilane; trifluoroacetic acid; for 0.5h;

DOI:10.1016/S0960-894X(03)00497-9

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