1,6-Dioxaspiro[4.5]decan-2-methal

Base Information

• Chemical Name: 1,6-Dioxaspiro[4.5]decan-2-methal
• CAS No.: 83015-88-7
• Molecular Formula: C9H16O3
• Molecular Weight: 172.22200
• Hs Code.: 2932999099
• Mol file: 83015-88-7.mol

Synonyms:1,6-dioxaspiro<4.5>decane-2-ylmethanol;1,6-Dioxaspiro

Chemical Property of 1,6-Dioxaspiro[4.5]decan-2-methal

Chemical Property:

• PSA: 38.69000
• LogP: 1.05450
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1,6-Dioxaspiro[4.5]decan-2-Methanol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-Dioxaspiro[4.5]decan-2-methal

There total 7 articles about 1,6-Dioxaspiro[4.5]decan-2-methal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1,6-Dioxaspiro<4.5>decan-2-carboxaldehyd (933685-24-6) → 1,6-Dioxaspiro<4.5>decan-2-methanol (83015-88-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1h; Ambient temperature;

DOI:10.1002/cber.19811140419

Reference yield:

1,7-dioxaspiro<5.5>undec-2-ene (78013-58-8) → 1,6-Dioxaspiro<4.5>decan-2-methanol (83015-88-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) BH₃, 2.) alkaline hydrogen peroxide / 1.) THF

2: 0.08 h / 140 °C

With alkaline hydrogen peroxide; borane;

DOI:10.1039/c39820000601

Reference yield:

2-(chloromethyl)tetrahydropyran (18420-41-2,130233-13-5,130233-14-6) → 1,6-Dioxaspiro<4.5>decan-2-methanol (83015-88-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 79 percent / KOH / 12 h / Heating

2: 72 percent / hydroquinone / 144 h / Ambient temperature

3: 82 percent / 85percent m-chloroperbenzoic acid / methanol / 1) -5 deg C, 2 h, 2) r.t., 1.5 h

4: 60 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

With potassium hydroxide; lithium aluminium tetrahydride; hydroquinone; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether;

DOI:10.1002/cber.19811140419

upstream raw materials:

(3S,6S)- and (3R,6R)-1,7-dioxaspiro<5.5>undecan-3-ol

1,6-Dioxaspiro<4.5>decan-2-carboxaldehyd

(3S,6S)-(+)-3-hydroxy-1,7-dioxaspiro<5.5>undecane

(3R,6S)-3-Hydroxy-1,7-dioxaspiro<5.5>undecane

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