Technology Process of C27H27N5
There total 6 articles about C27H27N5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 18 h / 20 °C
2: water; potassium carbonate / tetrahydrofuran; methanol / 60 °C
With
water; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.035
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 15 h / 20 °C
2: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 18 h / 20 °C
3: water; potassium carbonate / tetrahydrofuran; methanol / 60 °C
With
palladium 10% on activated carbon; water; hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2011.01.035