1,2-DINMETHOXY-PHENYL 4-O-BETA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: 1,2-DINMETHOXY-PHENYL 4-O-BETA-D-GLUCOPYRANOSIDE
• CAS No.: 84812-00-0
• Molecular Formula: C14H20O8
• Molecular Weight: 316.308
• Mol file: 84812-00-0.mol

Synonyms:Phenethyl |A-D-Glucopyranoside;Phenylethyl 2-Glucoside;|A-Phenylethyl |A-D-Glucoside;2-Phenylethyl |A-D-Glucoside;3,4-Dimethoxyphenyl Beta-D-glucopyranoside;|A-Phenylethanol Glucoside;Phenethyl |A-D-Glucoside;

Chemical Property of 1,2-DINMETHOXY-PHENYL 4-O-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

• PSA: 117.84000
• LogP: -1.11750
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

3,4-Dimethoxyphenylbeta-D-Glucoside 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-DINMETHOXY-PHENYL 4-O-BETA-D-GLUCOPYRANOSIDE

There total 6 articles about 1,2-DINMETHOXY-PHENYL 4-O-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-(3,4-dimethoxy-phenoxy)-tetrahydro-pyran-4-yl ester (136112-51-1) → 3,4-dimethoxybenzyl alcohol O-β-D-glucopyranoside (84812-00-0)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2016.05.017

Reference yield:

3,4-dimethoxyphenol (2033-89-8) → 3,4-dimethoxybenzyl alcohol O-β-D-glucopyranoside (84812-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 4 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

2: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;

DOI:10.1016/j.tetlet.2016.05.017

Reference yield:

2-Methoxyhydroquinone 4-O-<6-O-(4-O-α-L-rhamnopyranosyl)-syringyl>-β-D-glucopyranoside (136112-50-0) → 3,4-dimethoxybenzyl alcohol O-β-D-glucopyranoside (84812-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 38 mg / K₂CO₃ / Ambient temperature

2: 37 mg / diethyl ether

With potassium carbonate; In diethyl ether;

DOI:10.1248/cpb.39.865

upstream raw materials:

diazomethane

tachioside

2-Methoxyhydroquinone 4-O-<6-O-(4-O-α-L-rhamnopyranosyl)-syringyl>-β-D-glucopyranoside

2,3,4,6-tetra-O-acetyl-d-glucopyranosyl trichloroacetimidate

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