1-Oxo-2--1,2,3,4-tetrahydro-phenanthren

Base Information

• Chemical Name: 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren
• CAS No.: 102948-89-0
• Molecular Formula: C₂₆H₂₀O
• Molecular Weight: 348.444

Synonyms:

Chemical Property of 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren

There total 5 articles about 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-biphenylacetonitrile (31603-77-7) → 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren (102948-89-0)

Guidance literature:

Multi-step reaction with 3 steps

2: aq. H₂O₂, AcOH

3: (i) PCl₅, (ii) AlCl₃

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01066a012

Reference yield:

methyl 4-phenylbenzoate (720-75-2) → 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren (102948-89-0)

Guidance literature:

Multi-step reaction with 6 steps

1: LiAlH₄

2: aq. HBr

5: aq. H₂O₂, AcOH

6: (i) PCl₅, (ii) AlCl₃

With lithium aluminium tetrahydride; hydrogen bromide; dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01066a012

Reference yield:

p-phenylbenzyl bromide (2567-29-5) → 1-Oxo-2--1,2,3,4-tetrahydro-phenanthren (102948-89-0)

Guidance literature:

Multi-step reaction with 4 steps

3: aq. H₂O₂, AcOH

4: (i) PCl₅, (ii) AlCl₃

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01066a012

upstream raw materials:

2--4--buttersaeure

4-biphenylacetonitrile

methyl 4-phenylbenzoate

p-phenylbenzyl bromide

Downstream raw materials:

1-Hydroxy-2--1.2.3.4-tetrahydro-phenanthren

2-(Biphenylyl-⁽⁴⁾)-3,4-dihydro-phenanthren

2-(Biphenylyl-⁽⁴⁾)-phenanthren

2--phenantrachino

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