2-fluoro-N-phenylbenzenecarbothioamide

Base Information

Chemical Name:2-fluoro-N-phenylbenzenecarbothioamide
CAS No.:2027-54-5
Molecular Formula:C13H10 F N S
Molecular Weight:231.294
Hs Code.:
NSC Number:51894
DSSTox Substance ID:DTXSID30397854

Synonyms:2027-54-5;2-FLUORO-N-PHENYLBENZOTHIOAMIDE;2-fluoro-N-phenylbenzenecarbothioamide;NSC51894;DTXSID30397854;NSC-51894

Suppliers and Price of 2-fluoro-N-phenylbenzenecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 2-fluoro-N-phenylbenzenecarbothioamide

Chemical Property:

Vapor Pressure:0.000145mmHg at 25°C
Boiling Point:332.6°C at 760 mmHg
Flash Point:154.9°C
Density:1.282g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:231.05179866
Heavy Atom Count:16
Complexity:238

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=S)C2=CC=CC=C2F

Technology Process of 2-fluoro-N-phenylbenzenecarbothioamide

There total 4 articles about 2-fluoro-N-phenylbenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1747-80-4
2-fluoro-N-phenylbenzamide

: 2027-54-5
2-fluoro-N-phenyl-thiobenzamide

Guidance literature:: With Lawessons reagent; In toluene; at 100 ℃; Heating;
DOI:10.1016/j.tetlet.2008.05.100

Reference yield:

: 62-53-3
aniline

: 2027-54-5
2-fluoro-N-phenyl-thiobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: Lawessons reagent / toluene / 2 h / Reflux; Inert atmosphere

With Lawessons reagent; triethylamine; In dichloromethane; toluene;
DOI:10.1021/acs.orglett.8b03679

Reference yield:

: 393-52-2
2-Fluorobenzoyl chloride

: 2027-54-5
2-fluoro-N-phenyl-thiobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: Lawessons reagent / toluene / 2 h / Reflux; Inert atmosphere

With Lawessons reagent; triethylamine; In dichloromethane; toluene;
DOI:10.1021/acs.orglett.8b03679