C₄₀H₄₆F₂N₂O₆Si

Base Information

Chemical Name:C₄₀H₄₆F₂N₂O₆Si
CAS No.:950599-00-5
Molecular Formula:C₄₀H₄₆F₂N₂O₆Si
Molecular Weight:716.897
Hs Code.:

C<sub>40</sub>H<sub>46</sub>F<sub>2</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₄₀H₄₆F₂N₂O₆Si

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Technology Process of C₄₀H₄₆F₂N₂O₆Si

There total 11 articles about C₄₀H₄₆F₂N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 855248-38-3
3,4-bis-(4-fluoro-phenyl)-5-formyl-1-isopropyl-1H-pyrrole-2-carboxylic acid

: 950599-00-5
C₄₀H₄₆F₂N₂O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 80 °C

2: Et₃N / tetrahydrofuran / 12 h / 25 °C

3: toluene / 48 h / 110 °C

With thionyl chloride; triethylamine; In tetrahydrofuran; toluene; 3: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096

Reference yield:

: 1027038-69-2
C₂₁H₁₆ClF₂NO₂

: 950599-00-5
C₄₀H₄₆F₂N₂O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 12 h / 25 °C

2: toluene / 48 h / 110 °C

With triethylamine; In tetrahydrofuran; toluene; 2: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096

Reference yield:

: C₁₄H₉F₂NO₂

: 950599-00-5
C₄₀H₄₆F₂N₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: 38 percent / DBU / tetrahydrofuran / 12 h / 25 °C

2: 62 percent / KOH / dimethylsulfoxide / 1.5 h / 25 °C

3: 45 percent / POCl₃ / 1,2-dichloro-ethane / 3 h / 80 °C

4: 100 percent / NaOH / methanol / 2 h / 60 °C

5: SOCl₂ / 80 °C

6: Et₃N / tetrahydrofuran / 12 h / 25 °C

7: toluene / 48 h / 110 °C

With potassium hydroxide; sodium hydroxide; thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene; 1: Barton-Zard reaction / 3: Vilsmeir-Haack reaction / 7: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096