p-Menth-1-ene-3,6-diol

Base Information

• Chemical Name: p-Menth-1-ene-3,6-diol
• CAS No.: 4031-55-4
• Molecular Formula: C10H18O2
• Molecular Weight: 170.24900
• Mol file: 4031-55-4.mol

Synonyms:2-Cyclohexene-1,4-diol, 2-methyl-5-(1-methylethyl)-, [1S-(1α,4α,5β)]-;p-Menth-6-ene-2,5-diol, (2S,4R,5R)- (8CI);2-Cyclohexene-1,4-diol, 2-methyl-5-(1-methylethyl)-, (1S,4R,5R)-;(1S,4R,5R)-2-Methyl-5-(1-methylethyl)-2-cyclohexene-1,4-diol;

Chemical Property of p-Menth-1-ene-3,6-diol

Chemical Property:

• Melting Point: 165 °C
• Boiling Point: 279.4±40.0 °C(Predicted)
• PKA: 14.44±0.70(Predicted)
• PSA: 40.46000
• Density: 1.039±0.06 g/cm3(Predicted)
• LogP: 1.33040

Purity/Quality:

98%min ^*data from raw suppliers

p-Menth-1-ene-3,6-diol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of p-Menth-1-ene-3,6-diol

There total 6 articles about p-Menth-1-ene-3,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

(+)-(1R,4S,7R)-7-isopropyl-5-methyl-2,3-dioxabicyclo[2.2.2]oct-5-ene (114612-55-4) → (3R,4R,6S)-3,6-dihydroxymenth-1-ene (4031-53-2,4031-54-3,4031-56-5,17699-07-9,38301-95-0,61664-34-4,78037-71-5,143562-45-2,4031-55-4,676268-01-2)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1016/S0031-9422(96)00863-1

Reference yield:

(R)-5-isopropyl-2-methylcyclohexa-1,3-diene (4221-98-1) → (3R,4R,6S)-3,6-dihydroxymenth-1-ene (4031-53-2,4031-54-3,4031-56-5,17699-07-9,38301-95-0,61664-34-4,78037-71-5,143562-45-2,4031-55-4,676268-01-2)

Guidance literature:

With water; oxygen; at 70 ℃;

DOI:10.1016/S0040-4020(01)98658-2

Reference yield:

(R)-5-isopropyl-2-methylcyclohexa-1,3-diene (4221-98-1) → (3R,4R,6S)-3,6-dihydroxymenth-1-ene (4031-53-2,4031-54-3,4031-56-5,17699-07-9,38301-95-0,61664-34-4,78037-71-5,143562-45-2,4031-55-4,676268-01-2) + (1S,2S,5R)-2-methyl-5-(propan-2-yl)cyclohex-3-ene-1,2-diol (4031-52-1)

Guidance literature:

at 35 - 40 ℃; Durchleiten von Sauerstoff;

DOI:10.1039/jr9490002040

upstream raw materials:

(R)-5-isopropyl-2-methylcyclohexa-1,3-diene

(+)-(1R,4S,7R)-7-isopropyl-5-methyl-2,3-dioxabicyclo[2.2.2]oct-5-ene

Downstream raw materials:

(4R)-3t.6t-diacetoxy-1-methyl-4r-isopropyl-cyclohexene-⁽¹⁾

(1S:2S:4R:5S)-p-menthanediol-(2.5)

(+)-(1S,3S,4R,6S)-6-hydroxymenthol

thymoquinone

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