ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate

Base Information

Chemical Name:ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate
CAS No.:691902-34-8
Molecular Formula:C₂₇H₃₀O₄
Molecular Weight:418.533
Hs Code.:

Synonyms:

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Chemical Property of ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate

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Technology Process of ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate

There total 8 articles about ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 691905-26-7
2',6'-dimethyl-[1,1'-biphenyl]-3-carbaldehyde

: 691902-34-8
ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; 1,2-dimethoxyethane / 6 h / 0 - 20 °C

2: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran

With sodium tetrahydroborate; tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; 1,2-dimethoxyethane; 2: Mitsunobu reaction;
DOI:10.1021/jm101405t

Reference yield:

: C₁₄H₁₈O₅

: 691902-34-8
ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol; water / 20 °C

2: hydrogenchloride; water / ethanol / 0.5 h / Reflux

3: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran

With hydrogenchloride; tributylphosphine; palladium 10% on activated carbon; water; hydrogen; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; ethanol; water; 3: Mitsunobu reaction;
DOI:10.1021/jm101405t

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 691902-34-8
ethyl 3-[4-[(2',6'-dimethylbiphenyl-3-yl)methoxy]-2-methoxyphenyl]propionate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 20 h / 80 °C / Inert atmosphere

2: sodium tetrahydroborate / tetrahydrofuran; 1,2-dimethoxyethane / 6 h / 0 - 20 °C

3: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; sodium carbonate; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; toluene; 3: Mitsunobu reaction;
DOI:10.1021/jm101405t