(R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate

Base Information

Chemical Name:(R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate
CAS No.:204244-68-8
Molecular Formula:C₁₁H₁₃NO₂
Molecular Weight:191.23
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate

Chemical Property:

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Technology Process of (R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate

There total 4 articles about (R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 17285-57-3,144635-02-9,517907-57-2
1-(2-pyridinyl)but-3-en-1-ol

: 108-05-4,9003-20-7
vinyl acetate

: 517907-57-2
(S)-(-)-1-(pyridin-2-yl)but-3-en-1-ol

: 517907-57-2
(R)-1-(pyridin-2-yl)but-3-en-1-ol

: 204244-68-8
(R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate

Guidance literature:: With Pseudomonas cepacia lipase immobilized on modified ceramic; In tetrahydrofuran; at 24 ℃; for 30h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(02)00743-7

Reference yield:

: 17285-57-3,144635-02-9,517907-57-2
1-(2-pyridinyl)but-3-en-1-ol

: 108-05-4,9003-20-7
vinyl acetate

: 517907-57-2
(S)-(-)-1-(pyridin-2-yl)but-3-en-1-ol

: 204244-68-8
(R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate

Guidance literature:: With Pseudomonas cepacia PS-C Amona II lipase; In tetrahydrofuran; at 24 ℃; for 30h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Enzymatic reaction;
DOI:10.1016/j.tetasy.2010.02.016

Reference yield:

: 17285-57-3,144635-02-9,517907-57-2
1-(2-pyridinyl)but-3-en-1-ol

: 108-05-4,9003-20-7
vinyl acetate

: 517907-57-2
(S)-(-)-1-(pyridin-2-yl)but-3-en-1-ol

: 517907-57-2
(R)-1-(pyridin-2-yl)but-3-en-1-ol

: (S)-1-(2-pyridyl)but-3-en-1-yl acetate

: 204244-68-8
(R)-(+)-1-(pyridin-2-yl)but-3-enyl acetate

Guidance literature:: With 4 A molecular sieve; In di-isopropyl ether; at 60 ℃; for 72h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Candida antarctica lipase presence;
DOI:10.1021/jo971521g