trans-[Mo(CO)4(PPh₃)2] * 1,4-bis(diphenylphosphino)-2,5-difluorobenzene

Base Information

• Chemical Name: trans-[Mo(CO)4(PPh₃)2] * 1,4-bis(diphenylphosphino)-2,5-difluorobenzene
• CAS No.: 186180-49-4
• Molecular Formula: C₃₀H₂₂F₂P₂*C₄₀H₃₀MoO₄P₂
• Molecular Weight: 1215.01
• Mol file: 186180-49-4.mol

Synonyms:

Chemical Property of trans-[Mo(CO)4(PPh₃)2] * 1,4-bis(diphenylphosphino)-2,5-difluorobenzene

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of trans-[Mo(CO)4(PPh₃)2] * 1,4-bis(diphenylphosphino)-2,5-difluorobenzene

There total 1 articles about trans-[Mo(CO)4(PPh₃)2] * 1,4-bis(diphenylphosphino)-2,5-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

[Mo(CO)4(μ-1,4-bis(diphenylphosphino)-2,5-difluorobenzene)]2 + triphenylphosphine (603-35-0) → trans-[Mo(CO)4(PPh3)2] * 1,4-bis(diphenylphosphino)-2,5-difluorobenzene (186180-49-4)

Guidance literature:

With acetonitrile; In acetonitrile; refluxing Mo-complex for 4 h, cooling to room temp., addn. of 2 equiv. PPh3, stirring for 12 h; removal of volatiles (reduced pressure), extn. into CH2Cl2, solvent removal (reduced pressure), washing (light petroleum), crystn. on MeOH diffusion into CH2Cl2 soln.; elem. anal.;

DOI:10.1016/S0020-1693(96)05133-X

upstream raw materials:

triphenylphosphine