17,37-bis(4-[(10,15,20-triphenylporphinato)Zinc(II)-5-yl]phenylcarbonylamino)-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1⁽³⁸⁾,15⁽²⁰⁾,16,18,34,36-hexene

Base Information

• Chemical Name: 17,37-bis(4-[(10,15,20-triphenylporphinato)Zinc(II)-5-yl]phenylcarbonylamino)-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1⁽³⁸⁾,15⁽²⁰⁾,16,18,34,36-hexene
• CAS No.: 732282-50-7
• Molecular Formula: C₁₂₀H₁₀₀N₁₂O₁₀Zn₂
• Molecular Weight: 2000.97
• Mol file: 732282-50-7.mol

Synonyms:

Chemical Property of 17,37-bis(4-[(10,15,20-triphenylporphinato)Zinc(II)-5-yl]phenylcarbonylamino)-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1⁽³⁸⁾,15⁽²⁰⁾,16,18,34,36-hexene

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 17,37-bis(4-[(10,15,20-triphenylporphinato)Zinc(II)-5-yl]phenylcarbonylamino)-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1⁽³⁸⁾,15⁽²⁰⁾,16,18,34,36-hexene

There total 1 articles about 17,37-bis(4-[(10,15,20-triphenylporphinato)Zinc(II)-5-yl]phenylcarbonylamino)-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1⁽³⁸⁾,15⁽²⁰⁾,16,18,34,36-hexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

17,37-bis[4-(10,15,20-triphenyl-21H,23H-porphine-5-yl)phenylcarbonylamino]-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1(38),15(20),16,18,34,36-hexene + zinc(II) acetate dihydrate (5970-45-6) → 17,37-bis(4-[(10,15,20-triphenylporphinato)Zinc(II)-5-yl]phenylcarbonylamino)-21,33-dimethyl-2,5,8,11,14,24,27,30-octaoxa-21,33-diazatricyclo[32.4.0.0(15,20)]octatriaconta-1(38),15(20),16,18,34,36-hexene (732282-50-7)

Guidance literature:

In methanol; dichloromethane; addn. of a soln. of zinc salt in methanol to a soln. of ligand in CH2Cl2, stirring for 12 h at room temp.; addn. of water, extn. with CH2Cl2, evapn. of org. phase, washing with methanol; elem. anal.;

DOI:10.1039/b701317e

upstream raw materials:

zinc(II) acetate dihydrate