Technology Process of 1-(3-hydroxypentyl)cyclohexan-1-ol
There total 6 articles about 1-(3-hydroxypentyl)cyclohexan-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phenylsilane; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
for 24h;
regioselective reaction;
Reflux;
DOI:10.1002/anie.201501729
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis(acetylacetonate)oxovanadium; tert.-butylhydroperoxide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2: phenylsilane; tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / Reflux
With
tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; phenylsilane; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201501729
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis(cyclopentadienyl)titanium dichloride; manganese; C3H9ClSi*C3H10Si
2: nickel(II) acetate tetrahydrate; sodium tetrahydroborate; ethylenediamine; hydrogen / methanol / 12 h / 20 °C / Inert atmosphere; Schlenk technique
3: bis(acetylacetonate)oxovanadium; tert.-butylhydroperoxide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
4: phenylsilane; tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / Reflux
With
tert.-butylhydroperoxide; bis(cyclopentadienyl)titanium dichloride; manganese; sodium tetrahydroborate; bis(acetylacetonate)oxovanadium; C3H9ClSi*C3H10Si; phenylsilane; tetrabutyl ammonium fluoride; hydrogen; nickel(II) acetate tetrahydrate; ethylenediamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201501729
