4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

Base Information

Chemical Name:4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose
CAS No.:122901-35-3
Molecular Formula:C₄₈H₅₇NO₁₈
Molecular Weight:935.976
Hs Code.:

4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

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Chemical Property of 4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

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Technology Process of 4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

There total 5 articles about 4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 122901-34-2
3-O-acetyl-4-<1D-(1N,2,4,5/3,6)-(6-O-acetyl-2,3,4,5-tetra-O-benzyl-5-C-benzyloxymethyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,6-anhydro-2-O-benzyl-4-desoxy-β-D-glucopyranose

: 108-24-7
acetic anhydride

: 122901-35-3,122999-53-5
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

Guidance literature:: With boron trifluoride diethyl etherate; for 4h; Ambient temperature;

Reference yield:

: 106989-01-9
1L-2-azido-1,4,5,6-tetra-O-benzyl-2-desoxy-4-C-(benzyloxymethyl)-muco-inosit

: 122901-35-3,122999-53-5
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / NaBH₄ / 4 percent NiCl₂ / ethanol

2: propan-1-ol / 30 h / 90 °C

3: pyridine

4: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

With pyridine; sodium tetrahydroborate; boron trifluoride diethyl etherate; nickel dichloride; In propan-1-ol; ethanol;

Reference yield:

: 33208-46-7
1,6:3,4-Dianhydro-2-O-benzyl-β-D-galactopyranose

: 122901-35-3,122999-53-5
4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,6-tri-O-acetyl-4,5-di-O-benzyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-1,3,6-tri-O-acetyl-2-O-benzyl-4-desoxy-α,β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: propan-1-ol / 30 h / 90 °C

2: pyridine

3: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; In propan-1-ol;