C₅₇H₆₃NO₁₂

Base Information

Chemical Name:C₅₇H₆₃NO₁₂
CAS No.:1380244-29-0
Molecular Formula:C₅₇H₆₃NO₁₂
Molecular Weight:954.127
Hs Code.:

C<sub>57</sub>H<sub>63</sub>NO<sub>12</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₇H₆₃NO₁₂

Chemical Property:

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Technology Process of C₅₇H₆₃NO₁₂

There total 6 articles about C₅₇H₆₃NO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₇H₆₁NO₁₂

: 1380244-29-0
C₅₇H₆₃NO₁₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -78 °C / Molecular sieve

2: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C

3: potassium tri-sec-butyl-borohydride / -78 - -30 °C

With triethylsilane; oxalyl dichloride; trifluorormethanesulfonic acid; potassium tri-sec-butyl-borohydride; triethylamine; In dichloromethane; dimethyl sulfoxide; 2: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033

Reference yield:

: 1380244-28-9
C₅₇H₆₃NO₁₂

: 1380244-29-0
C₅₇H₆₃NO₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C

2: potassium tri-sec-butyl-borohydride / -78 - -30 °C

With oxalyl dichloride; potassium tri-sec-butyl-borohydride; triethylamine; In dichloromethane; dimethyl sulfoxide; 1: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033

Reference yield:

: C₃₇H₄₅NO₁₆

: 1380244-29-0
C₅₇H₆₃NO₁₂

Guidance literature:: Multi-step reaction with 5 steps

1: water; triethylamine / methanol / 4 h / 40 °C

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 °C

3: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -78 °C / Molecular sieve

4: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / -60 - -30 °C

5: potassium tri-sec-butyl-borohydride / -78 - -30 °C

With triethylsilane; oxalyl dichloride; trifluorormethanesulfonic acid; water; sodium hydride; potassium tri-sec-butyl-borohydride; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: Zemplen deacetylation / 4: Swern oxidation;
DOI:10.1016/j.carres.2012.03.033