rhodium⁽¹⁺⁾-[(1,2,5,6)-1,5-cyclooctadiene]-[2-[(1-methylthio-S)-3-[(diphenylphosphino-P)oxy]propyl]-N,N-dimethyl-benzenamine]-tetrafluoroborate^(1-)

Base Information

• Chemical Name: rhodium⁽¹⁺⁾-[(1,2,5,6)-1,5-cyclooctadiene]-[2-[(1-methylthio-S)-3-[(diphenylphosphino-P)oxy]propyl]-N,N-dimethyl-benzenamine]-tetrafluoroborate^(1-)
• CAS No.: 749850-13-3
• Molecular Formula: BF₄*C₃₂H₄₀NOPRhS
• Molecular Weight: 707.426

Synonyms:

Chemical Property of rhodium⁽¹⁺⁾-[(1,2,5,6)-1,5-cyclooctadiene]-[2-[(1-methylthio-S)-3-[(diphenylphosphino-P)oxy]propyl]-N,N-dimethyl-benzenamine]-tetrafluoroborate^(1-)

Chemical Property:

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Useful:

Technology Process of rhodium⁽¹⁺⁾-[(1,2,5,6)-1,5-cyclooctadiene]-[2-[(1-methylthio-S)-3-[(diphenylphosphino-P)oxy]propyl]-N,N-dimethyl-benzenamine]-tetrafluoroborate^(1-)

There total 1 articles about rhodium⁽¹⁺⁾-[(1,2,5,6)-1,5-cyclooctadiene]-[2-[(1-methylthio-S)-3-[(diphenylphosphino-P)oxy]propyl]-N,N-dimethyl-benzenamine]-tetrafluoroborate^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate + 2-[1-methylthio-3-[(diphenylphosphino)oxy]propyl]-N,N-dimethyl-benzenamine (591214-27-6) → rhodium(1+)-[(1,2,5,6)-1,5-cyclooctadiene]-[2-[(1-methylthio-S)-3-[(diphenylphosphino-P)oxy]propyl]-N,N-dimethyl-benzenamine]-tetrafluoroborate(1-) (749850-13-3)

Guidance literature:

In dichloromethane; under Ar atm. soln. ligand in CH2Cl2 was added dropwise to soln. (Rh(COD)2)BF4 in CH2Cl2 with dry ice/acetone cooling bath, react. mixt. was warmed slowly to room temp. withing 1 h and stirred for 2 h; soln. was concd. in vacuo, ether was added, ppt. was washed with ether and dried; elem. anal.;

DOI:10.1016/j.ica.2004.02.005

upstream raw materials:

2-[1-methylthio-3-[(diphenylphosphino)oxy]propyl]-N,N-dimethyl-benzenamine

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