[Ni(4-aminoacetophenone thiosemicarbazone)2(SO₄)]

Base Information

• Chemical Name: [Ni(4-aminoacetophenone thiosemicarbazone)2(SO₄)]
• CAS No.: 873660-17-4
• Molecular Formula: C₁₈H₂₄N₈NiO₄S₃
• Molecular Weight: 571.328

Synonyms:

Chemical Property of [Ni(4-aminoacetophenone thiosemicarbazone)2(SO₄)]

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Technology Process of [Ni(4-aminoacetophenone thiosemicarbazone)2(SO₄)]

There total 1 articles about [Ni(4-aminoacetophenone thiosemicarbazone)2(SO₄)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(E)-2-(1-(4-aminophenyl)ethylidene)hydrazinecarbothioamide + nickel(II) sulfate hydrate → [Ni(4-aminoacetophenone thiosemicarbazone)2(SO4)] (873660-17-4)

Guidance literature:

In ethanol; water; a hot (ca. 75°C) aq. ethanolic soln. (1:1, v/v) of Ni-contg. compd. (0.05 mol) and a hot ethanolic soln. of a ligand (0.1 mol) were mixedwith stirring; the mixt. was refluxed for ca. 5 h at ca. 80°C; c ooling to ca. 5°C; the complex was filtered, washed with 50 % ethanol and dried over P4O10 under vac.; elem. anal.;

DOI:10.1016/j.saa.2005.04.005

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