Os(P(C₆H₅)3)2(CO)2HCl

Base Information

Chemical Name:Os(P(C₆H₅)3)2(CO)2HCl
CAS No.:54933-53-8
Molecular Formula:C₃₈H₃₁ClO₂OsP₂
Molecular Weight:807.263
Hs Code.:

Os(P(C<sub>6</sub>H<sub>5</sub>)3)2(CO)2HCl

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os(P(C₆H₅)3)2(CO)2HCl

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Technology Process of Os(P(C₆H₅)3)2(CO)2HCl

There total 6 articles about Os(P(C₆H₅)3)2(CO)2HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

: 307498-17-5,83076-12-4
Os(κ2(C,P)-C6H4PPh2)H(CO)2(triphenylphosphine)

: 54933-53-8,25702-67-4
Os(P(C₆H₅)3)2(CO)2HCl

Guidance literature:: With HCl; In ethanol; dichloromethane; water; refluxed for 30 min; CH2Cl2 removed, crystals filtered, washed with EtOH;
DOI:10.1016/S0022-328X(00)81212-7

Reference yield: 93.0%

: 16971-31-6,36007-23-5
OsHCl(CO)(triphenylphosphine)₃

: 25702-67-4,54933-53-8
dicarbonylchlorohydridobis(triphenylphosphine)osmium(II)

Guidance literature:: With carbon monoxide; In benzene; High Pressure; Os complex in benzene pressurizing with 3 atm CO, stirring for 2 h at 25°C, filtering, reducing in volume, EtOH adding, ppt. filtering off, washing with Et2O; purified by recrystallisation from benzene/EtOH; identified by elem. anal., IR and NMR spectra;
DOI:10.1016/S0020-1693(00)83666-X

Reference yield:

: 79725-76-1
osmium (ethylene)(carbonyl)2(triphenylphosphine)2

: 54933-53-8,25702-67-4
Os(P(C₆H₅)3)2(CO)2HCl

Guidance literature:: Multi-step reaction with 2 steps

1: tert-butyl alcohol

2: HCl / water; ethanol; dichloromethane

With HCl; In ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/S0022-328X(00)81212-7