C₃₆H₄₆N₈O₅S

Base Information

Chemical Name:C₃₆H₄₆N₈O₅S
CAS No.:1421639-74-8
Molecular Formula:C₃₆H₄₆N₈O₅S
Molecular Weight:702.878
Hs Code.:

C<sub>36</sub>H<sub>46</sub>N<sub>8</sub>O<sub>5</sub>S

Synonyms:

Suppliers and Price of C₃₆H₄₆N₈O₅S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₆H₄₆N₈O₅S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₆H₄₆N₈O₅S

There total 19 articles about C₃₆H₄₆N₈O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₄N₂O₃

: 1421639-74-8
C₃₆H₄₆N₈O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid; water / dichloromethane / 0.5 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.5 h

With water; sodium hydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm3016987

Reference yield:

: 214750-77-3
N-α-(9-fluoromethoxycarbonyl)-L-4-tert-butoxycarbonylaminophenylalanine

: 1421639-74-8
C₃₆H₄₆N₈O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); N-ethyl-N,N-diisopropylamine / dichloromethane

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.17 h

3.1: triethylamine / dichloromethane / 14 h

4.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 2 h / 0 - 20 °C / Inert atmosphere

6.1: trifluoroacetic acid; water / dichloromethane / 0.5 h / 20 °C

7.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

8.1: trifluoroacetic acid / dichloromethane / 0.5 h

With lithium aluminium tetrahydride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); water; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm3016987

Reference yield:

: 95753-55-2,177966-63-1
N-α-FMOC-4-nitro-L-phenylalanine

: 1421639-74-8
C₃₆H₄₆N₈O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: palladium 10% on activated carbon; ammonium formate / methanol / 14 h / 20 °C

2.1: sodium hydrogencarbonate / water; 1,4-dioxane / 14 h / 0 - 20 °C

3.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); N-ethyl-N,N-diisopropylamine / dichloromethane

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.17 h

5.1: triethylamine / dichloromethane / 14 h

6.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C / Inert atmosphere

8.1: trifluoroacetic acid; water / dichloromethane / 0.5 h / 20 °C

9.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

10.1: trifluoroacetic acid / dichloromethane / 0.5 h

With lithium aluminium tetrahydride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); palladium 10% on activated carbon; water; ammonium formate; sodium hydride; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm3016987