tert-butyl octahydropyrrolo[3,2-c]pyridine-1-carboxylate

Base Information

• Chemical Name: tert-butyl octahydropyrrolo[3,2-c]pyridine-1-carboxylate
• CAS No.: 848410-13-9
• Molecular Formula: C12H22N2O2
• Molecular Weight: 226.31500
• Hs Code.: 2933990090
• Mol file: 848410-13-9.mol

Synonyms:1-BOC-OCTAHYDROPYRROLO[3,2-C]PYRIDINE;PBN20111051;TERT-BUTYL OCTAHYDROPYRROLO[3,2-C]PYRIDINE-1-CARBOXYLATE;

Chemical Property of tert-butyl octahydropyrrolo[3,2-c]pyridine-1-carboxylate

Chemical Property:

• PSA: 41.57000
• LogP: 1.87200

Purity/Quality:

97% ^*data from raw suppliers

1-Boc-octahydropyrrolo[3,2-c]pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl octahydropyrrolo[3,2-c]pyridine-1-carboxylate

There total 11 articles about tert-butyl octahydropyrrolo[3,2-c]pyridine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate (148760-75-2) → tert-butyl octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate (1147422-00-1,848410-13-9)

Guidance literature:

With 10 wt% Pd(OH)2 on carbon; hydrogen; acetic acid; In 2-methoxy-ethanol; at 70 ℃; for 24h; under 15001.5 Torr;

Reference yield: 99.0%

5-benzyl-octahydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester (1147421-99-5) → tert-butyl octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate (1147422-00-1,848410-13-9)

Guidance literature:

With hydrogen; 5% palladium hydroxide on activated carbon; In methanol; ethanol; at 20 ℃; for 10h;

Reference yield: 42.0%

tert-butyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate (148760-75-2) → tert-butyl rac-(3aR,7aS)-octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate (848410-13-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; acetic acid; at 20 ℃; for 72h; under 2585.81 Torr;

upstream raw materials:

tert-butyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate

5-azaindole

3-methyl-4-nitropyridine N-oxide

di-tert-butyl dicarbonate

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