Technology Process of C69H86FNO18
There total 5 articles about C69H86FNO18 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrazine acetate / dimethylformamide / 1 h / 50 °C
2: 0.11 g / DBU / CH2Cl2 / 0.5 h / 0 °C
3: 1) 4 Angstroem molecular sieves, 2) trimethylsilyl triflate / 1) CH2Cl2, 0 deg C, 30 min, 2) CH2Cl2, 50 min
4: ethylenediamine, 3 Angstroem molecular sieves / butan-1-ol / Heating
5: 76.2 mg / pyridine
With
pyridine; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; 4 A molecular sieve; hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; ethylenediamine;
In
dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1016/S0008-6215(96)00266-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethylenediamine, 3 Angstroem molecular sieves / butan-1-ol / Heating
2: 76.2 mg / pyridine
With
pyridine; 3 A molecular sieve; ethylenediamine;
In
butan-1-ol;
DOI:10.1016/S0008-6215(96)00266-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 0.11 g / DBU / CH2Cl2 / 0.5 h / 0 °C
2: 1) 4 Angstroem molecular sieves, 2) trimethylsilyl triflate / 1) CH2Cl2, 0 deg C, 30 min, 2) CH2Cl2, 50 min
3: ethylenediamine, 3 Angstroem molecular sieves / butan-1-ol / Heating
4: 76.2 mg / pyridine
With
pyridine; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; 4 A molecular sieve; 1,8-diazabicyclo[5.4.0]undec-7-ene; ethylenediamine;
In
dichloromethane; butan-1-ol;
DOI:10.1016/S0008-6215(96)00266-2
