(R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)

Base Information

Chemical Name:(R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)
CAS No.:1374428-93-9
Molecular Formula:C₂₄H₁₆Br₂O₅
Molecular Weight:544.196
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)

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Technology Process of (R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)

There total 3 articles about (R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1374428-90-6
(R)-8-deoxyscytalone

: 586-75-4
4-chlorobenzoyl chloride

: 1374428-93-9
(R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.1002/anie.201107695

Reference yield:

: 59079-32-2
1,3,6-trihydroxynaphthalene

: 1374428-93-9
(R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: glucose dehydrogenase; 17β-hydroxysteroid dehydrogenase of Cochliobolus lunatus; D-glucose; β-nicotinamide adenine dinucleotide phosphate sodium salt / 24 h / pH 7 / KPi buffer; Inert atmosphere; Enzymatic reaction

2: pyridine / 4 h / 20 °C

With glucose dehydrogenase; pyridine; D-glucose; 17β-hydroxysteroid dehydrogenase of Cochliobolus lunatus; β-nicotinamide adenine dinucleotide phosphate sodium salt;
DOI:10.1002/anie.201107695

Reference yield:

: 20349-39-7
4-hydroxy-2,7-naphthalenedisulfonic acid disodium salt

: 1374428-93-9
(R)-4-oxo-1,2,3,4-tetrahydronaphthalene-2,7-diyl bis(4-bromobenzoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / 0.5 h / 250 - 290 °C

1.2: pH 1

2.1: glucose dehydrogenase; 17β-hydroxysteroid dehydrogenase of Cochliobolus lunatus; D-glucose; β-nicotinamide adenine dinucleotide phosphate sodium salt / 24 h / pH 7 / KPi buffer; Inert atmosphere; Enzymatic reaction

3.1: pyridine / 4 h / 20 °C

With glucose dehydrogenase; pyridine; D-glucose; 17β-hydroxysteroid dehydrogenase of Cochliobolus lunatus; β-nicotinamide adenine dinucleotide phosphate sodium salt; sodium hydroxide;
DOI:10.1002/anie.201107695