C₂₀H₃₃O₁₃P₃Si

Base Information

Chemical Name:C₂₀H₃₃O₁₃P₃Si
CAS No.:1446517-59-4
Molecular Formula:C₂₀H₃₃O₁₃P₃Si
Molecular Weight:602.481
Hs Code.:

C<sub>20</sub>H<sub>33</sub>O<sub>13</sub>P<sub>3</sub>Si

Synonyms:

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Chemical Property of C₂₀H₃₃O₁₃P₃Si

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Technology Process of C₂₀H₃₃O₁₃P₃Si

There total 2 articles about C₂₀H₃₃O₁₃P₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1777-03-3
2-triethylsilylacetylene

: 1428631-89-3
C₁₂H₁₈IO₁₃P₃

: 1446517-59-4
C₂₀H₃₃O₁₃P₃Si

Guidance literature:: With copper(l) iodide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; triethylamine; In water; acetonitrile; at 20 - 55 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja312148q

Reference yield:

: 1428631-86-0
C₁₂H₁₅IO₄

: 1446517-59-4
C₂₀H₃₃O₁₃P₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethyl phosphite; trichlorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / -15 - 10 °C / Inert atmosphere

1.2: 0.5 h / -10 - 0 °C

2.1: trisodium tris(3-sulfophenyl)phosphine; copper(l) iodide; palladium diacetate; triethylamine / water; acetonitrile / 0.5 h / 20 - 55 °C / Inert atmosphere

With trimethyl phosphite; copper(l) iodide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; trichlorophosphate; In water; acetonitrile; 2.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja312148q