dibenzyl heptathiotricarbonate

Base Information

• Chemical Name: dibenzyl heptathiotricarbonate
• CAS No.: 1422636-50-7
• Molecular Formula: C₁₇H₁₄S₇
• Molecular Weight: 442.76
• Mol file: 1422636-50-7.mol

Synonyms:

Chemical Property of dibenzyl heptathiotricarbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibenzyl heptathiotricarbonate

There total 2 articles about dibenzyl heptathiotricarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophosgene (463-71-8) + potassium benzyl carbonotrithioate (62907-90-8) → tetrabenzyl (1,3-dithietane-2,2,4,4-tetrayl)tetracarbonotrithioate (1422636-47-2) + dibenzyl heptathiotricarbonate (1422636-50-7)

Guidance literature:

In diethyl ether; for 1.25h; Cooling with ice;

DOI:10.1016/j.tet.2012.12.053

Reference yield:

phenylmethanethiol (100-53-8) → tetrabenzyl (1,3-dithietane-2,2,4,4-tetrayl)tetracarbonotrithioate (1422636-47-2) + dibenzyl heptathiotricarbonate (1422636-50-7)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / tetrahydrofuran

2: diethyl ether / 1.25 h / Cooling with ice

With potassium hydroxide; In tetrahydrofuran; diethyl ether;

DOI:10.1016/j.tet.2012.12.053

upstream raw materials:

thiophosgene

potassium benzyl carbonotrithioate

phenylmethanethiol