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Technology Process of CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2

CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2

Base Information
  • Chemical Name:CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2
  • CAS No.:1272520-27-0
  • Molecular Formula:C27H28Cl2N2OZr
  • Molecular Weight:558.662
  • Hs Code.:
CpZr[OC<sub>9</sub>H<sub>5</sub>NCHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2]Cl<sub>2</sub>

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Chemical Property of CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2
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Technology Process of CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2

There total 1 articles about CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

cyclopentadienylzirconium trichloride

cyclopentadienylzirconium trichloride

2-{[(2,6-diisopropylphenyl)imino]methyl}quinolin-8-ol
948300-19-4

2-{[(2,6-diisopropylphenyl)imino]methyl}quinolin-8-ol

CpZr[OC<sub>9</sub>H<sub>5</sub>NCHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2]Cl<sub>2</sub>
1272520-27-0

CpZr[OC9H5NCHNC6H3(CH(CH3)2)2]Cl2

Guidance literature:
With NaH; In tetrahydrofuran; byproducts: NaCl; (Ar); ligand added dropwise at 0°C to a suspn. of NaH, stirred for 2 h at room temp., filtered, the filtrate cooled to -78°C and added dropwise to a soln. of Zr complex, warmed to room temp. and stirredovernight; evapd. (vac.), extd. (toluene), evapd. (vac.), recrystd. (toluene/pentane); elem. anal.;
DOI:10.1021/om101059v
upstream raw materials:

2-{[(2,6-diisopropylphenyl)imino]methyl}quinolin-8-ol

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