{((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}

Base Information

Chemical Name:{((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}
CAS No.:157109-11-0
Molecular Formula:C₂₅H₂₉Cl₂O₂PRu
Molecular Weight:564.454
Hs Code.:

{((CH<sub>3</sub>)2CHC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(O)OCH<sub>3</sub>)RuCl<sub>2</sub>}

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Chemical Property of {((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}

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Technology Process of {((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}

There total 2 articles about {((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 32744-65-3
Diphenylphosphinoessigsaeuremethylester

: 157109-11-0
{((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}

Guidance literature:: In dichloromethane; under N2 or Ar; stirring for 20 h; addn. of Et2O, washing (Et2O), drying, elem. anal.;
DOI:10.1016/0022-328X(94)88129-4

Reference yield: 64.0%

: {((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OC(CH₃)3)RuCl₂}*0.25CHCl₃

: 157109-11-0
{((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}

Guidance literature:: With sulfuric acid; In methanol; dichloromethane; under N2 or Ar; dissolving Ru-complex in CH2Cl2, addn. of a soln. of H2SO4 in methanol, stirring for 3 d; concg. under reduced pressure, filtn., washing (ethanol and then Et2O), detn. by IR and NMR;;
DOI:10.1016/0022-328X(94)88129-4

Reference yield: 55.0%

: ammonium hexafluorophosphate

: 75-18-3
dimethylsulfide

: 157109-11-0
{((CH₃)2CHC₆H₄CH₃)((C₆H₅)2PCH₂C(O)OCH₃)RuCl₂}

: 157109-31-4
{((CH₃)2CHC₆H₄CH₃)((CH₃)2S)((C₆H₅)2PCH₂C(O)OCH₃)ClRu}⁽¹⁺⁾*PF₆^(1-)={(C₁₀H₁₄)((CH₃)2S)((C₆H₅)2PCH₂C(O)OCH₃)RuCl}PF₆

Guidance literature:: In methanol; dichloromethane; under N2 or Ar; stirring for 24 h; removing solvents (vac.), extn. of residue (CH2Cl2), filtn., addn. of additional Me2S to the filtrate, covering with Et2O, elem. anal.;
DOI:10.1016/0022-328X(94)88129-4