Technology Process of C18H27IO3
There total 8 articles about C18H27IO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole; iodine; triphenylphosphine;
In
toluene;
at 20 ℃;
for 12.1667h;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 7 steps
1: magnesium chloride; triethylamine / tetrahydrofuran / 20 °C
2: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
4: copper dichloride; water / acetonitrile / Reflux
5: sodium tetrahydroborate / ethanol / 0 °C
6: hydrogen; palladium on activated charcoal; sodium hydrogencarbonate / ethanol / 3 h / 20 °C
7: triphenylphosphine; iodine; 1H-imidazole / toluene / 12.17 h / 20 °C
With
1H-imidazole; sodium tetrahydroborate; di-isopropyl azodicarboxylate; palladium on activated charcoal; potassium tert-butylate; water; hydrogen; iodine; sodium hydrogencarbonate; triethylamine; triphenylphosphine; copper dichloride; magnesium chloride;
In
tetrahydrofuran; ethanol; toluene; acetonitrile;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen; palladium on activated charcoal; sodium hydrogencarbonate / ethanol / 3 h / 20 °C
2: triphenylphosphine; iodine; 1H-imidazole / toluene / 12.17 h / 20 °C
With
1H-imidazole; palladium on activated charcoal; hydrogen; iodine; sodium hydrogencarbonate; triphenylphosphine;
In
ethanol; toluene;
DOI:10.1021/ja4018122
