C₁₂H₁₅N₃

Base Information

Chemical Name:C₁₂H₁₅N₃
CAS No.:1332955-37-9
Molecular Formula:C₁₂H₁₅N₃
Molecular Weight:201.271
Hs Code.:

C<sub>12</sub>H<sub>15</sub>N<sub>3</sub>

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Suppliers and Price of C₁₂H₁₅N₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₅N₃

Chemical Property:

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Technology Process of C₁₂H₁₅N₃

There total 4 articles about C₁₂H₁₅N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353369-80-8
(E)-6-phenylhex-3-en-1-yl 4-methylbenzenesulfonate

: 1332955-37-9
C₁₂H₁₅N₃

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo201027u

Reference yield:

: 67280-87-9,64025-65-6
(E)-6-(phenyl)hex-3-en-1-ol

: 1332955-37-9
C₁₂H₁₅N₃

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

With dmap; sodium azide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo201027u

Reference yield:

: 16520-62-0
4-Phenyl-1-butyne

: 1332955-37-9
C₁₂H₁₅N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium amide; ferric nitrate / diethyl ether / 1 h / -78 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: ammonia; sodium / tetrahydrofuran / 8 h / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

With dmap; sodium azide; lithium amide; ammonia; sodium; ferric nitrate; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo201027u