Technology Process of Methyl-[2-methylaminomethyl-6-(1,1,2,2-tetrafluoro-2-phenyl-ethyl)-benzyl]-amine
There total 4 articles about Methyl-[2-methylaminomethyl-6-(1,1,2,2-tetrafluoro-2-phenyl-ethyl)-benzyl]-amine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: (i) Mg, Et2O, (ii) /BRN= 1932620/, (iii) aq. citric acid
2: aq. H2SeO3 / dioxane / Heating
3: SF4, Hg, HF / benzene
4: NBS, (PhCO)2O2 / CCl4 / Heating
With
N-Bromosuccinimide; sulfur tetrafluoride; hydrogen fluoride; selenious acid; mercury; dibenzoyl peroxide;
In
1,4-dioxane; tetrachloromethane; benzene;
DOI:10.1021/jm00213a021
- Guidance literature:
-
Multi-step reaction with 3 steps
1: SF4, Hg, HF / benzene
2: NBS, (PhCO)2O2 / CCl4 / Heating
With
N-Bromosuccinimide; sulfur tetrafluoride; hydrogen fluoride; mercury; dibenzoyl peroxide;
In
tetrachloromethane; benzene;
DOI:10.1021/jm00213a021
- Guidance literature:
-
Multi-step reaction with 5 steps
1: (i) Mg, Et2O, (ii) /BRN= 1932620/, (iii) aq. citric acid
2: aq. H2SeO3 / dioxane / Heating
3: SF4, Hg, HF / benzene
4: NBS, (PhCO)2O2 / CCl4 / Heating
With
N-Bromosuccinimide; sulfur tetrafluoride; hydrogen fluoride; selenious acid; mercury; dibenzoyl peroxide;
In
1,4-dioxane; tetrachloromethane; benzene;
DOI:10.1021/jm00213a021
