CH₃C₆H₄CO₂Cu(P(C₆H₅)3)2

Base Information

• Chemical Name: CH₃C₆H₄CO₂Cu(P(C₆H₅)3)2
• CAS No.: 32335-62-9
• Molecular Formula: C₄₄H₃₇CuO₂P₂
• Molecular Weight: 723.27
• Mol file: 32335-62-9.mol

Synonyms:

Chemical Property of CH₃C₆H₄CO₂Cu(P(C₆H₅)3)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of CH₃C₆H₄CO₂Cu(P(C₆H₅)3)2

There total 1 articles about CH₃C₆H₄CO₂Cu(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-tolylcopper (20854-03-9) → CH3C6H4CO2Cu(P(C6H5)3)2 (32335-62-9) + [(triphenylphosphine)2Cu(HCO3)] (73716-93-5)

Guidance literature:

With triphenylphosphine; carbon dioxide; In toluene; addn. of triphenylphosphine to stirred suspn. of Cu-compd. under dry nitrogen at 0°C, the deep-orange soln. formed was filtered and CO2 bubbled through it for a few hours, HOCO2Cu(PPh3)2 sepd. spontaneously from soln.; o-TCO2Cu(PPh3)2 pptd. by adding ether to the previously concd. soln., elem. anal.;

DOI:10.1016/S0022-328X(00)95267-7

Reference yield:

CH3C6H4CO2Cu(P(C6H5)3)2 (32335-62-9) → [(Ph3P)2Cu(κ2-O2CH)] (265311-26-0,32335-51-6)

Guidance literature:

In 1,2-dimethoxyethane; reflux;

DOI:10.1016/S0022-328X(00)95267-7

upstream raw materials:

o-tolylcopper

Downstream raw materials:

[(Ph₃P)₂Cu(κ²-O₂CH)]