Technology Process of C32H35N7O2S
There total 4 articles about C32H35N7O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-methyl-pyrrolidin-2-one / Heating
2: aluminum (III) chloride / dichloromethane
With
aluminum (III) chloride;
In
1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/ml300110s
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 18 h / 20 °C
2.1: triethylamine; magnesium chloride / acetonitrile / 0.25 h / -10 - 0 °C
2.2: 0.25 h
2.3: 1.5 h / Reflux
3.1: 1-methyl-pyrrolidin-2-one / Heating
4.1: aluminum (III) chloride / dichloromethane
With
aluminum (III) chloride; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; magnesium chloride;
In
1-methyl-pyrrolidin-2-one; dichloromethane; acetonitrile;
DOI:10.1021/ml300110s
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; magnesium chloride / acetonitrile / 0.25 h / -10 - 0 °C
1.2: 0.25 h
1.3: 1.5 h / Reflux
2.1: 1-methyl-pyrrolidin-2-one / Heating
3.1: aluminum (III) chloride / dichloromethane
With
aluminum (III) chloride; triethylamine; magnesium chloride;
In
1-methyl-pyrrolidin-2-one; dichloromethane; acetonitrile;
DOI:10.1021/ml300110s