BOC-LEU-(R)-VAL-OH

Base Information

• Chemical Name: BOC-LEU-(R)-VAL-OH
• CAS No.: 82252-39-9
• Molecular Formula: C16H32N2O4
• Molecular Weight: 316.43600
• Mol file: 82252-39-9.mol

Synonyms:N-<2(S)-<(tert-butyloxycarbonyl)amino>-4-methylpentyl>-L-valine;Boc-Leu-()-Val-OH;BOC-LEU-Y-[CH2NH]-VAL-OH;N-{2(S)-[(tert-butyloxycarbony)amino]-4-methylpentyl}-L-valine;BOC-LEU-(R)-VAL-OH;

Chemical Property of BOC-LEU-(R)-VAL-OH

Chemical Property:

• PSA: 87.66000
• LogP: 3.40640
• Storage Temp.: -15°C

Purity/Quality:

98%Min ^*data from raw suppliers

Boc-Leu-psi(CH2NH)Val-OH 95%-98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOC-LEU-(R)-VAL-OH

There total 3 articles about BOC-LEU-(R)-VAL-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nα-Boc-LeuΨVal-OBzl (82252-38-8) → N-<2(S)-<(tert-butyloxycarbony)amino>-4-methylpentyl>-L-valine (82252-39-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; under 2068.6 Torr;

DOI:10.1021/jm00396a006

Reference yield:

N-tert-butoxycarbonyl-L-leucine (13139-15-6,53296-34-7) → N-<2(S)-<(tert-butyloxycarbony)amino>-4-methylpentyl>-L-valine (82252-39-9)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / Pd/C / 2068.6 Torr

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jm00396a006

Reference yield:

L-valine benzyl ester (21760-98-5) → N-<2(S)-<(tert-butyloxycarbony)amino>-4-methylpentyl>-L-valine (82252-39-9)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / Pd/C / 2068.6 Torr

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jm00396a006

upstream raw materials:

N^α-Boc-LeuΨVal-OBzl

N-tert-butoxycarbonyl-L-leucine

L-valine benzyl ester

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