C₆H₅PbC₆H₃(C₆H₂(C₃H₇)3)2

Base Information

• Chemical Name: C₆H₅PbC₆H₃(C₆H₂(C₃H₇)3)2
• CAS No.: 287406-57-9
• Molecular Formula: C₄₂H₅₄Pb
• Molecular Weight: 766.091

Synonyms:

Chemical Property of C₆H₅PbC₆H₃(C₆H₂(C₃H₇)3)2

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Technology Process of C₆H₅PbC₆H₃(C₆H₂(C₃H₇)3)2

There total 1 articles about C₆H₅PbC₆H₃(C₆H₂(C₃H₇)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[Pb(μ-Br)(C6H3-2,6-(2,4,6-C6H2-(i-Pr)3)2)]2 + phenyllithium (591-51-5) → C6H5PbC6H3(C6H2(C3H7)3)2 (287406-57-9)

Guidance literature:

In diethyl ether; byproducts: LiBr; a Et2O soln. of PhLi was added to a stirred soln. of Pb-compound in Et2O at -78°C, stirred for 1 h and allowed to warm to room temp. (N2atm.); the solvent was removed under reduced pressure, ppt. was extd. with benzene, filtered, reduced in vol., stored at .approx. 4°C; elem. anal.;

DOI:10.1021/om0001624

upstream raw materials:

phenyllithium

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