C₃₄H₃₉N₅O₅S

Base Information

Chemical Name:C₃₄H₃₉N₅O₅S
CAS No.:1332639-49-2
Molecular Formula:C₃₄H₃₉N₅O₅S
Molecular Weight:629.78
Hs Code.:

C<sub>34</sub>H<sub>39</sub>N<sub>5</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₃₄H₃₉N₅O₅S

Chemical Property:

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Technology Process of C₃₄H₃₉N₅O₅S

There total 29 articles about C₃₄H₃₉N₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1332639-49-2
C₃₄H₃₉N₅O₅S

Guidance literature:: Multi-step reaction with 13 steps

1.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 - 45 °C

3.1: dmap / dichloromethane / 3 h / 0 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

5.1: sodium periodate / ruthenium(III) trichloride hydrate / 1-methyl-pyrrolidin-2-one; tetrachloromethane; acetonitrile; water / 3.83 h

6.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1.5 h / 0 °C

6.2: 4 h / 0 - 20 °C

7.1: Lawessons reagent / toluene / 1.5 h / 50 °C

8.1: ethanol / 1 h / Reflux

9.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

10.1: HATU / 1-methyl-pyrrolidin-2-one

11.1: trifluoroacetic acid / dichloromethane

12.1: HATU / 1-methyl-pyrrolidin-2-one

13.1: trifluoroacetic acid / dichloromethane

With Lawessons reagent; dmap; sodium periodate; tetrabutyl ammonium fluoride; chloroformic acid ethyl ester; sodium hydride; triethylamine; HATU; trifluoroacetic acid; ruthenium(III) trichloride hydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 187039-57-2,335280-19-8
(2S,3S)-1-(tert-butoxycarbonyl)-3-hydroxypyrrolidine-2-carboxylic acid

: 1332639-49-2
C₃₄H₃₉N₅O₅S

Guidance literature:: Multi-step reaction with 21 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 90 °C

2.1: 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C

3.1: lithium borohydride / tetrahydrofuran / 3 h / 0 - 20 °C

4.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 - 20 °C

5.1: triethylamine / 12 h

6.1: thionyl chloride / dichloromethane / 1 h / -78 °C

6.2: 1 h / -78 °C

7.1: / acetonitrile / 16 h / 20 °C

8.1: hydrogen / ethanol / 1.5 h / 2585.81 Torr

9.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 - 45 °C

11.1: dmap / dichloromethane / 3 h / 0 °C

12.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

13.1: sodium periodate / ruthenium(III) trichloride hydrate / 1-methyl-pyrrolidin-2-one; tetrachloromethane; acetonitrile; water / 3.83 h

14.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1.5 h / 0 °C

14.2: 4 h / 0 - 20 °C

15.1: Lawessons reagent / toluene / 1.5 h / 50 °C

16.1: ethanol / 1 h / Reflux

17.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

18.1: HATU / 1-methyl-pyrrolidin-2-one

19.1: trifluoroacetic acid / dichloromethane

20.1: HATU / 1-methyl-pyrrolidin-2-one

21.1: trifluoroacetic acid / dichloromethane

With Lawessons reagent; 1H-imidazole; dmap; sodium periodate; lithium borohydride; thionyl chloride; tetrabutyl ammonium fluoride; hydrogen; sulfur trioxide pyridine complex; chloroformic acid ethyl ester; sodium hydride; potassium carbonate; triethylamine; HATU; trifluoroacetic acid; ruthenium(III) trichloride hydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; tetrachloromethane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 184046-78-4
(2S,3S)-1-tert-butyl-2-methyl 3-hydroxypyrrolidine-1,2-dicarboxylate

: 1332639-49-2
C₃₄H₃₉N₅O₅S

Guidance literature:: Multi-step reaction with 20 steps

1.1: 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 3 h / 0 - 20 °C

3.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 - 20 °C

4.1: triethylamine / 12 h

5.1: thionyl chloride / dichloromethane / 1 h / -78 °C

5.2: 1 h / -78 °C

6.1: / acetonitrile / 16 h / 20 °C

7.1: hydrogen / ethanol / 1.5 h / 2585.81 Torr

8.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 - 45 °C

10.1: dmap / dichloromethane / 3 h / 0 °C

11.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

12.1: sodium periodate / ruthenium(III) trichloride hydrate / 1-methyl-pyrrolidin-2-one; tetrachloromethane; acetonitrile; water / 3.83 h

13.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1.5 h / 0 °C

13.2: 4 h / 0 - 20 °C

14.1: Lawessons reagent / toluene / 1.5 h / 50 °C

15.1: ethanol / 1 h / Reflux

16.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

17.1: HATU / 1-methyl-pyrrolidin-2-one

18.1: trifluoroacetic acid / dichloromethane

19.1: HATU / 1-methyl-pyrrolidin-2-one

20.1: trifluoroacetic acid / dichloromethane

With Lawessons reagent; 1H-imidazole; dmap; sodium periodate; lithium borohydride; thionyl chloride; tetrabutyl ammonium fluoride; hydrogen; sulfur trioxide pyridine complex; chloroformic acid ethyl ester; sodium hydride; triethylamine; HATU; trifluoroacetic acid; ruthenium(III) trichloride hydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; tetrachloromethane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile;