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Technology Process of [Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6

[Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6

Base Information
  • Chemical Name:[Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6
  • CAS No.:330804-73-4
  • Molecular Formula:C6H6*C24H46Ni2P4Si4
  • Molecular Weight:766.36
  • Hs Code.:
[Ni((SiH<sub>2</sub>)C<sub>6</sub>H<sub>4</sub>(SiH))((P(CH<sub>3</sub>)2CH<sub>2</sub>)2)]2*C<sub>6</sub>H<sub>6</sub>

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Chemical Property of [Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6
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Technology Process of [Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6

There total 2 articles about [Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

[Ni((SiH<sub>2</sub>)2C<sub>6</sub>H<sub>4</sub>)((P(CH<sub>3</sub>)2CH<sub>2</sub>)2)P(CH<sub>2</sub>)2CH<sub>2</sub>]2

[Ni((SiH2)2C6H4)((P(CH3)2CH2)2)P(CH2)2CH2]2

[Ni((SiH<sub>2</sub>)C<sub>6</sub>H<sub>4</sub>(SiH))((P(CH<sub>3</sub>)2CH<sub>2</sub>)2)]2*C<sub>6</sub>H<sub>6</sub>
330804-73-4

[Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6

Guidance literature:
In (2)H8-toluene; 110°C, 30 min; crystn. (C6H6);
DOI:10.1002/1521-3773(20010105)40:1<213::AID-ANIE213>3.0.CO;2-W

Reference yield: 34.0%

[Ni((SiH<sub>2</sub>)2C<sub>6</sub>H<sub>4</sub>)((P(CH<sub>3</sub>)2CH<sub>2</sub>)2)P(CH<sub>2</sub>)2CH<sub>2</sub>]2

[Ni((SiH2)2C6H4)((P(CH3)2CH2)2)P(CH2)2CH2]2

benzene
71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1

benzene

[Ni((SiH<sub>2</sub>)C<sub>6</sub>H<sub>4</sub>(SiH))((P(CH<sub>3</sub>)2CH<sub>2</sub>)2)]2*C<sub>6</sub>H<sub>6</sub>
330804-73-4

[Ni((SiH2)C6H4(SiH))((P(CH3)2CH2)2)]2*C6H6

Guidance literature:
In toluene; under N2; heated at 110°C, 30 min; evapd. (vac., 1E-4 Torr); crystd. by slow cooling of hot benzene soln. to room temp. after a few seed crystals were added; liquid removed; washed (C6H6, Et2O); dried (vac.); solid manually separated under a microscope from precursor; elem. anal.;
DOI:10.1002/1521-3773(20010105)40:1<213::AID-ANIE213>3.0.CO;2-W
upstream raw materials:

benzene

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