(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal

Base Information

Chemical Name:(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal
CAS No.:1187629-81-7
Molecular Formula:C₂₉H₄₄O₆
Molecular Weight:488.665
Hs Code.:

(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal

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Chemical Property of (2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal

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Technology Process of (2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal

There total 1 articles about (2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187629-80-6
(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentan-1-ol

: 1187629-81-7
(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal

Guidance literature:: (2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentan-1-ol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -55 ℃; for 1h; Inert atmosphere;

With triethylamine; In dichloromethane; at -55 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo9012833

Reference yield:

: 1187629-81-7
(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal

: 42333-37-9
(2E,4E)-6-(diethoxyphosphoryl)hexa-2,4-dienoic acid ethyl ester

: 1187629-64-6
(2E,4E,6E,8S,9R,10R)-ethyl 9-methoxy-10-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-8-methylundeca-2,4,6-trienoate

Guidance literature:: (2E,4E)-6-(diethoxyphosphoryl)hexa-2,4-dienoic acid ethyl ester; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

(2S,3R,4R)-3-methoxy-4-((4R,5S,6R)-6-((2E,4E)-6-(4-methoxybenzyloxy)-4-methylhexa-2,4-dien-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)-2-methylpentanal; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/jo9012833