trans-[FeH(N₂)(1,2-bis(diphenylphosphino)ethane)2]BPh₄ C₂₄H₂₀B^(1-)*C₅₂H₄₉FeN₂P₄⁽¹⁺⁾, yellow

Base Information

• Chemical Name: trans-[FeH(N₂)(1,2-bis(diphenylphosphino)ethane)2]BPh₄ C₂₄H₂₀B^(1-)*C₅₂H₄₉FeN₂P₄⁽¹⁺⁾, yellow
• CAS No.: 38831-75-3
• Molecular Formula: C₂₄H₂₀B*C₅₂H₄₉FeN₂P₄
• Molecular Weight: 1200.95
• Mol file: 38831-75-3.mol

Synonyms:

Chemical Property of trans-[FeH(N₂)(1,2-bis(diphenylphosphino)ethane)2]BPh₄ C₂₄H₂₀B^(1-)*C₅₂H₄₉FeN₂P₄⁽¹⁺⁾, yellow

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-[FeH(N₂)(1,2-bis(diphenylphosphino)ethane)2]BPh₄ C₂₄H₂₀B^(1-)*C₅₂H₄₉FeN₂P₄⁽¹⁺⁾, yellow

There total 2 articles about trans-[FeH(N₂)(1,2-bis(diphenylphosphino)ethane)2]BPh₄ C₂₄H₂₀B^(1-)*C₅₂H₄₉FeN₂P₄⁽¹⁺⁾, yellow which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

[FeH(1,2-bis(diphenylphosphino)ethane)2]BPh4 (38928-62-0) + nitrogen (7727-37-9) → trans-[FeH(N2)(1,2-bis(diphenylphosphino)ethane)2]BPh4 C24H20B(1-)*C52H49FeN2P4(1+), yellow (38831-75-3)

Guidance literature:

In tetrahydrofuran; all manipulations under N2 atm.; soln. of complex stirred for 3 h under N2; solvent removed in vac., residue dissolved in CH2Cl2, pptd. with Et2O, filtered, dried in vac.;

DOI:10.1002/zaac.200500502

Reference yield:

[FeH(1,2-bis(diphenylphosphino)ethane)2]BPh4 (38928-62-0) + nitrogen (7727-37-9) → [FeH(N2)(1,2-bis(diphenylphosphino)ethane)2]BPh4 C24H20B(1-)*C52H49FeN2P4(1+), green (38831-75-3)

Guidance literature:

DOI:10.1002/zaac.200500502

upstream raw materials:

[FeH(1,2-bis(diphenylphosphino)ethane)2]BPh₄

nitrogen