1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

Base Information

Chemical Name:1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride
CAS No.:137898-41-0
Molecular Formula:10C₂₁H₂₂N₆O₂*11ClH
Molecular Weight:4305.52
Hs Code.:

1-<methyl(2-quinolinylmethyl)amino>-3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

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Chemical Property of 1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

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Technology Process of 1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

There total 8 articles about 1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 137915-52-7
1-(Methyl-quinolin-2-ylmethyl-amino)-3-[4-(1-trityl-1H-tetrazol-5-yl)-phenoxy]-propan-2-ol

: 137898-41-0
1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

Guidance literature:: With hydrogenchloride; for 3h;
DOI:10.1021/jm00115a010

Reference yield:

: 6926-51-8
5-(4-methoxyphenyl)-1H-tetrazole

: 137898-41-0
1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / Et₃N / dimethylformamide / 3 h / 70 °C

2: 42 percent / propanethiol, NaH / dimethylformamide / 80 °C

3: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, RT, 3 h

4: 35 percent / acetonitrile / Heating

5: 48 percent / ethanol. HCl / 3 h

With hydrogenchloride; 1-thiopropane; sodium hydride; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00115a010

Reference yield:

: 3747-74-8
2-(chloromethyl)quinoline monohydrochloride

: 137898-41-0
1--3-<4-(1H-tetrazol-5-yl)phenoxy>-2-propanol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / H₂O / 3.33 h / 10 - 20 °C

2: 35 percent / acetonitrile / Heating

3: 48 percent / ethanol. HCl / 3 h

With hydrogenchloride; In water; acetonitrile;
DOI:10.1021/jm00115a010