N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(S)-N-methyl-leucineanilide

Base Information

Chemical Name:N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(S)-N-methyl-leucineanilide
CAS No.:1412908-35-0
Molecular Formula:C₂₄H₃₃F₃N₄O₄
Molecular Weight:498.546
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(S)-N-methyl-leucineanilide

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Technology Process of N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(S)-N-methyl-leucineanilide

There total 1 articles about N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(S)-N-methyl-leucineanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

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: N-trifluoroacetyl-(S)-alanyl-glycyl-N-methyl-leucineanilide

: 70122-91-7
ethyl (2-methylallyl)carbonate

: 1412908-35-0
N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(S)-N-methyl-leucineanilide

: N-trifluoroacetyl-(S)-alanyl-(R)-(2-methylallyl)glycyl-(R)-N-methyl-leucineanilide

Guidance literature:: N-trifluoroacetyl-(S)-alanyl-glycyl-N-methyl-leucineanilide; With n-butyllithium; diisopropylamine; zinc(II) chloride; In tetrahydrofuran; at -78 - -40 ℃; for 0.75h; Schlenk technique;

ethyl (2-methylallyl)carbonate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; at -78 - 20 ℃; Overall yield = 70 %; Overall yield = 152 mg; diastereoselective reaction; Schlenk technique;
DOI:10.1039/c2ob26351c DOI:10.1039/c2ob26351c