C₃₇H₄₆O₅

Base Information

Chemical Name:C₃₇H₄₆O₅
CAS No.:1374425-57-6
Molecular Formula:C₃₇H₄₆O₅
Molecular Weight:570.769
Hs Code.:

C<sub>37</sub>H<sub>46</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₄₆O₅

Chemical Property:

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Technology Process of C₃₇H₄₆O₅

There total 25 articles about C₃₇H₄₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₅₀O₆

: 1374425-57-6
C₃₇H₄₆O₅

Guidance literature:: With lead(IV) tetraacetate; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/ejoc.201101629

Reference yield:

: C₁₃H₂₀O₅

: 1374425-57-6
C₃₇H₄₆O₅

Guidance literature:: Multi-step reaction with 20 steps

1.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

5.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

6.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

7.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

7.2: 0.5 h / -78 °C / Inert atmosphere

7.3: 5 h / -78 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

9.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

9.2: 3 h / -78 °C / Inert atmosphere

10.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

12.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

13.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

13.2: 0.5 h / -78 - 20 °C / Inert atmosphere

14.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

15.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

16.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

17.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / -50 °C / Inert atmosphere

17.2: 3 h / -50 °C / Inert atmosphere

18.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

19.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / tetrahydrofuran / Inert atmosphere

19.2: 5 h / 20 °C

20.1: lead(IV) tetraacetate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With pyridine; bis-triphenylphosphine-palladium(II) chloride; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; lead(IV) tetraacetate; palladium diacetate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629

Reference yield:

: 1374425-20-3
C₁₃H₂₀O₃

: 1374425-57-6
C₃₇H₄₆O₅

Guidance literature:: Multi-step reaction with 22 steps

1.1: triethylamine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: ozone / dichloromethane / 3 h / -78 °C

2.2: 4 h / 20 °C / Inert atmosphere

3.1: methanol; diethyl ether; toluene / 0.25 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / water; acetone / 0.5 h / 20 °C

7.1: triethylamine / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

8.1: oxygen; palladium diacetate / dimethyl sulfoxide / 16 h / 20 - 80 °C

9.1: iodine; magnesium / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

9.3: 5 h / -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / acetone / 0.5 h / 20 °C / Inert atmosphere

11.1: n-butyllithium; lithium diisopropyl amide / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

11.2: 3 h / -78 °C / Inert atmosphere

12.1: pyridine; dihydrogen peroxide / dichloromethane; water / 0.5 h / 0 - 20 °C

13.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.25 h / -78 °C / Inert atmosphere

14.1: 1,2-dichloro-benzene / 1 h / 220 °C / Microwave irradiation; Inert atmosphere

15.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

15.2: 0.5 h / -78 - 20 °C / Inert atmosphere

16.1: water; iodine / tetrahydrofuran / 16 h / 20 °C

17.1: triethyl borane; tri-n-butyl-tin hydride / hexane; toluene / 1 h / -78 °C / Air

18.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

19.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / -50 °C / Inert atmosphere

19.2: 3 h / -50 °C / Inert atmosphere

20.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

21.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / tetrahydrofuran / Inert atmosphere

21.2: 5 h / 20 °C

22.1: lead(IV) tetraacetate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With pyridine; bis-triphenylphosphine-palladium(II) chloride; lithium aluminium tetrahydride; n-butyllithium; triethyl borane; water; dihydrogen peroxide; iodine; oxygen; tri-n-butyl-tin hydride; lead(IV) tetraacetate; palladium diacetate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; ozone; magnesium; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; toluene; mineral oil;
DOI:10.1002/ejoc.201101629