C₁₆H₂₂N₂O₃

Base Information

Chemical Name:C₁₆H₂₂N₂O₃
CAS No.:1277191-49-7
Molecular Formula:C₁₆H₂₂N₂O₃
Molecular Weight:290.362
Hs Code.:

C<sub>16</sub>H<sub>22</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₂N₂O₃

Chemical Property:

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Technology Process of C₁₆H₂₂N₂O₃

There total 4 articles about C₁₆H₂₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1277191-53-3
C₁₆H₂₀N₄O₃

: 1277191-49-7
C₁₆H₂₂N₂O₃

Guidance literature:: With palladium 10% on activated carbon; hydrogen; sodium acetate; In ethyl acetate; at 20 ℃; for 4h;
DOI:10.1021/jo1021234

Reference yield:

: 1252614-32-6
C₁₆H₂₁NO₄

: 1277191-49-7
C₁₆H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 25 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 24 h / 80 °C

3: palladium 10% on activated carbon; hydrogen; sodium acetate / ethyl acetate / 4 h / 20 °C

With sodium azide; palladium 10% on activated carbon; hydrogen; sodium acetate; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo1021234

Reference yield:

: 1170175-59-3
(-)-(S)-N-tert-(butoxycarbonyl)-5-[(S)-hydroxy(phenyl)methyl]-1H-pyrrol-2(5H)-one

: 1277191-49-7
C₁₆H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen; sodium acetate / ethyl acetate / 4 h / 20 °C

2: triethylamine / dichloromethane / 0 - 25 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 24 h / 80 °C

4: palladium 10% on activated carbon; hydrogen; sodium acetate / ethyl acetate / 4 h / 20 °C

With sodium azide; palladium 10% on activated carbon; hydrogen; sodium acetate; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo1021234