Technology Process of C68H80N4O6S3
There total 4 articles about C68H80N4O6S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; XPhos / toluene; water / 6 h / 80 °C / Inert atmosphere
2: N-Bromosuccinimide / chloroform / 1 h / 20 °C / Inert atmosphere
3: potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; XPhos / toluene; water / 6 h / 80 °C / Inert atmosphere
4: triethylamine; piperidine; magnesium sulfate / dichloromethane / 40 °C / Inert atmosphere
With
piperidine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium phosphate; N-Bromosuccinimide; magnesium sulfate; triethylamine; XPhos;
In
dichloromethane; chloroform; water; toluene;
DOI:10.1039/c2cc35125k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; XPhos / toluene; water / 6 h / 80 °C / Inert atmosphere
2: N-Bromosuccinimide / chloroform / 1 h / 20 °C / Inert atmosphere
3: potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; XPhos / toluene; water / 6 h / 80 °C / Inert atmosphere
4: triethylamine; piperidine; magnesium sulfate / dichloromethane / 40 °C / Inert atmosphere
With
piperidine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium phosphate; N-Bromosuccinimide; magnesium sulfate; triethylamine; XPhos;
In
dichloromethane; chloroform; water; toluene;
DOI:10.1039/c2cc35125k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide / chloroform / 1 h / 20 °C / Inert atmosphere
2: potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; XPhos / toluene; water / 6 h / 80 °C / Inert atmosphere
3: triethylamine; piperidine; magnesium sulfate / dichloromethane / 40 °C / Inert atmosphere
With
piperidine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium phosphate; N-Bromosuccinimide; magnesium sulfate; triethylamine; XPhos;
In
dichloromethane; chloroform; water; toluene;
DOI:10.1039/c2cc35125k